X-Ray Diffuse Scattering
نویسنده
چکیده
In this research program, modern x-ray scattering techniques are used to study the structures and phase transitions in novel states of condensed matter. We have two principal experimental facilities. At M.I.T. we have three high-resolution computer controlled x-ray spectrometers using either a conventional or high intensity rotating anode x-ray generator. The angular resolution can be made as fine as 1.8 seconds of arc; this enables one to probe the development of order from distances of the order of the x-ray wavelength, ~1 A, up to 30,000 A. The sample temperature may be varied between 2 K and 500 K with a relative accuracy of 2 x 10-3K. We are currently installing a two spectrometer system at the National Synchrotron Light Source at Brookhaven National Laboratory. This makes possible high resolution scattering experiments with a flux more than three orders of magnitude larger than that from a rotating anode x-ray generator. This opens up a new generation of experiments. Synchrotron x-ray scattering experiments are also carried out on a wiggler beam line at the Stanford Synchrotron Radiation Laboratory.
منابع مشابه
Fully Atomistic Analysis of Diffuse X-ray Scattering Spectra of Silicon Defects
Diffuse X-ray scattering is a useful method for studying defects in silicon and metals. Although the traditional approaches of analyzing experimental diffuse X-ray scattering data have given much information about the size of defects and defect clusters, they are not very well suited for determining the atomic configuration. We present a fully atomistic computational method to calculate the dif...
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ABSTRACT Background: Coherent scattering leads to diffraction effects and especially constructive interferences. Theseinterferences carry some information about the molecular structure of the tissue. As breast cancer isthe most widespread cancer in women, this project evaluated the application of small angleX-ray scattering (SAXS) for differentiation between normal and cancerous breast tissues....
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Diffuse x-ray scattering is a powerful means to study the structure of defects in crystalline solids. The traditional analysis of diffuse x-ray scattering experiments relies on analytical and numerical methods which are not well suited for studying complicated defect configurations. We present here an atomistic simulation method by which the diffuse x-ray scattering can be calculated for an arb...
متن کاملDiffuse scattering in Ih ice.
Single crystals of ice Ih, extracted from the subglacial Lake Vostok accretion ice layer (3621 m depth) were investigated by means of diffuse x-ray scattering and inelastic x-ray scattering. The diffuse scattering was identified as mainly inelastic and rationalized in the frame of ab initio calculations for the ordered ice XI approximant. Together with Monte-Carlo modelling, our data allowed re...
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X-ray diffraction from macromolecular crystals includes both sharply peaked Bragg reflections and diffuse intensity between the peaks. The information in Bragg scattering reflects the mean electron density in the unit cells of the crystal. The diffuse scattering arises from correlations in the variations of electron density that may occur from one unit cell to another, and therefore contains in...
متن کاملPredicting X-ray diffuse scattering from translation–libration–screw structural ensembles
Identifying the intramolecular motions of proteins and nucleic acids is a major challenge in macromolecular X-ray crystallography. Because Bragg diffraction describes the average positional distribution of crystalline atoms with imperfect precision, the resulting electron density can be compatible with multiple models of motion. Diffuse X-ray scattering can reduce this degeneracy by reporting o...
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